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Basic Module in Bioorganic Chemistry

VAK 02-317-7-406

from January 8 to February 8, 2008

Instructors: Dr. Johannes Ranke (JR)
Prof. Dr. Detlef Gabel (DG)
Ulrike Bottin-Weber (UB)

Program

Date Time Room Topic Instructor
Tu, 08.01. 10:00 - 12:00 NW2 C0020 Introduction to reading a structural formula in 17 steps
Test
Safety instructions
DG
13:00 - 18:00 Lab Extraction of trimyristin from nutmeg
(pdf)
UB and JR
We, 9.01. 09:00 - 12:00 Lab Extraction of trimyristin from nutmeg UB and JR
13:00 - 15:00 UFT 2230 Mass Spectrometry JR
15:00 - 18:00 Lab Extraction of trimyristin from nutmeg JR
Th, 10.01. 08:30 - 09:30 UFT 0730 Short introduction to HPLC (pdf) JR
09:30 - 12:00 Lab Introductory HPLC experiments (pdf) UB and JR
Th, 10.01. 13:00 - 15:00 UFT 2230 General (Steps 1-4), Stereochemistry (Steps 5-7) DG
15:00 - 18:00 Lab Separation of aromatic compounds by HPLC-UV JR
Fr, 11.01. 10:00 - 12:30 Lab Nitration of benzaldehyde to 3-nitrobenzaldehyde UB and JR
13:30 - 15:00 UFT 2230 Introduction to Molecular interaction potentials JR
Tu, 15.01. 10:00 - 12:00 NW2 C0020 Noncovalent interaction potentials (Steps 8-13) DG
13:00 - 18:00 Lab Nitration of benzaldehyde to 3-nitrobenzaldehyde UB and JR
We, 16.01. 09:00 - 12:00 Lab Acid-catalyzed acetalization of 3-nitrobenzaldehyde with ethane diole UB and JR
13:00 - 15:00 UFT 2230 Reactivity (Steps 14-16) DG
15:00 - 18:00 Lab Acid-catalyzed acetalization of 3-nitrobenzaldehyde with ethane diole JR
Th, 17.01. 09:00 - 12:00 Lab Acid-catalyzed acetalization of 3-nitrobenzaldehyde with ethane diole UB and JR
13:00 - 15:00 UFT 2230 Functional Groups (Step 17) DG
15:00 - 18:00 Lab Acid-catalyzed acetalization of 3-nitrobenzaldehyde with ethane diole JR
Fr, 18.01. 10:00 - 15:00 Lab Kinetics of the reaction of selected isothiazol-3-ones with glutathione (pdf) UB and JR
15:00 - 17:00 UFT 2230 NMR Spectroscopy DG
Tu, 22.01. 10:00 - 12:00 NW2 C0020 IR Spectroscopy DG
13:00 - 18:00 Lab DG
We, 23.01. 09:00 - 12:00 Lab DG
13:00 - 15:00 UFT 2230 Hydrophobicity determination by reversed phase HPLC JR
15:00 - 18:00 Lab DG
Th, 24.01. 09:00 - 12:00 Lab DG
13:00 - 15:00 UFT 2230 UV/VIS Spectroscopy DG
15:00 - 18:00 Lab DG
Fr, 25.01. 10:00 - 12:00 Lab DG
13:00 - 15:00 UFT 2230 Fragment based methods for chemical property estimation JR
Tu, 29.01. 10:00 - 12:00 NW2 C0020 Lewis acids and bases, metal ions DG
13:00 - 18:00 Lab DG
We, 30.01. 09:00 - 12:00 Lab DG
13:00 - 15:00 UFT 2230 Modes of biocidal action JR
15:00 - 18:00 Lab DG
Th, 31.01. 09:00 - 12:00 Lab DG
13:00 - 15:00 UFT 2230 Measures and molecular descriptors of polarity JR
15:00 - 18:00 Lab DG
Fr, 01.02. 10:00 - 15:00 Lab DG
15:00 - 17:00 UFT 2230 Lecture DG
Tu, 05.02. 10:00 - 12:00 Lab DG
13:00 - 15:00 UFT 0730 Seminar talks DG and JR
15:00 - 18:00 Lab DG
We, 06.02. 09:00 - 15:00 Lab DG
15:00 - 17:00 UFT 2230 Seminar talks DG and JR
Th, 07.02. 09:00 - 12:00 Lab DG
13:00 - 15:00 UFT 2230 Cytochrome P450: Significance and reaction mechanisms JR
15:00 - 18:00 Lab DG
Fr, 08.02. 10:00 - 12:00 UFT 2230 Test, Wrap up DG and JR

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