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Basic Module in Bioorganic Chemistry

VAK 02-7903

from January 10 to February 10, 2006

Teachers: Prof. B. Jastorff
Prof. D. Gabel
Assistants: Jürgen Arning
Andrea Böschen
Ulrike Bottin-Weber
Anja Müller
Dr. Johannes Ranke
Stefan Stolte
Seminar topics: PDF document (27 kB)

Program

Date Time Room Topic Responsible
Tu, 10.01. 09:00 - 10:00 2230 Introductory seminar for the Basic Module in Bioorganic Chemistry Prof. Dr. B. Jastorff
10:00 - 12:00 2230 Time schedule of experiments, safety precautions, intro to the labs Dr. J. Ranke
13:00 - 15:00 2230 Introductory lecture for the Basic Module in Bioorganic Chemistry Prof. Dr. B. Jastorff
15:00 - 17:00 2230 Preparation of the first experiment
We, 11.01. 09:00 - 17:00 Lab Extraction of trimyristin from nutmeg
(pdf, small scale)
(pdf, bigger scale)
Anja Müller and Johannes Ranke
Th, 12.01. Lab Hydrolysis and MS-analysis of trimyristin Anja Müller and Johannes Ranke
Fr, 13.01. 10:30 - 12:00 2230 Lecture Prof. Dr. B. Jastorff
Fr, 13.01. 13:00 - 15:00 2230 Seminar Prof. Dr. B. Jastorff et al.
Tu, 17.01. 08:30 - 09:30 2230 Introduction to HPLC K. Thiele
Lab Introductory HPLC experiments U. Bottin-Weber and K. Thiele
We, 18.01. 08:30 - 09:30 0010 Separation in reversed-phase HPLC Prof. Dr. B. Jastorff
Lab Separation of aromatic compounds by HPLC-UV U. Bottin-Weber and K. Thiele
Th, 19.01. Lab Determination of Theobromine from Chocolate U. Bottin-Weber, A. Müller and K. Thiele
Fr, 20.01. 10:15 - 12:00 2230 Lecture Prof. Dr. B. Jastorff
13:00 - 14:00 2230 - Metabolism of xenobiotics within cells: Comparison of metabolic transformation pathways of benzene and toluene
- Toxicology and mechanism of action of Paraquat
Students
14:00 - 16:00 2230 Lecture Prof. Dr. B. Jastorff
Tu, 24.01. 08:30 - 09:30 2230 Seminar on Distillation (pdf) Stefan Stolte
Lab Distillation (pdf) Stefan Stolte
We, 25.01. 08:30 - 09:30 0010 Seminar on Synthesis of aspirin (pdf) Stefan Stolte
Lab Synthesis of aspirin (pdf) Stefan Stolte
Th, 26.01. 09:00 - 10:00 0010 Seminar on Acetalization of 3-nitrobenzaldehyde (pdf) Stefan Stolte
Th, 26.01. Lab Acid-catalyzed acetalization of 3-nitrobenzaldehyde with ethane diole (please look at both versions, alhough you will do only one) (pdf, 10 mmol) (pdf, 100 mmol) Stefan Stolte
Fr, 27.01. 10:15 - 12:00 2230 Lecture Prof. Dr. B. Jastorff
13:00 - 14:00 2230 - Mode of action of aspirin
- Effects of theobromine on humans: Biochemical mechanisms and their relation to its chemical structure
Students
Fr, 27.01. 14:15 - 16:00 2230 Seminar Prof. Dr. B. Jastorff
Tu, 31.01. 08:30 - 09:30 2230 Seminar J. Arning
Lab HPLC separation of cAMP metabolites J. Arning and U. Bottin-Weber
We, 01.02. 08:30 - 09:30 0010 Seminar J. Arning
Lab Kinetics of cAMP degradation in liver U. Bottin-Weber and J. Arning
Th, 02.02. Lab cAMP degradation in liver cell culture U. Bottin-Weber and J. Arning
Fr, 03.02. 10:15 - 12:00 2230 Lecture Prof. Dr. B. Jastorff
13:00 - 14:00 2230 - Common detection methods in HPLC
- Modes of liquid chromatography and related stationary phases (normal phase, reversed phase, ion exchange, ion pair chromatography)
Students
14:15 - 16:00 2230 Seminar Prof. Dr. B. Jastorff et al.
Tu, 07.02. 08:30 - 09:30 2230 Seminar S. Stolte
Lab Oxidation of oleic acid (pdf) A. Böschen and S. Stolte
We, 08.02. 08:30 - 09:30 0010 Seminar J. Ranke
Lab Preparation of a cAMP-analogue A. Müller and J. Ranke
Th, 09.02. Lab Purification and packaging of a cAMP-analogue A. Müller and J. Ranke
Fr, 10.02. 10:15 - 12:00 2230 Lecture Prof. Dr. B. Jastorff
13:00 - 17:00 2230 - Cyclic nucleotides in cell signalling processes (cAMP, cGMP, GTP)
- To be defined
Students
14:15 - 16:00 2230 Closing Seminar Prof. Dr. B. Jastorff et al.

vak_02-7903_en.html last modified on February 01, 2006